N,N-二甲基对甲苯磺酰胺合成路线 （共 34 条）
反应条件
water; trifluoroacetic acid T=99°C; determined by 1H NMR; Rate constant;
参考文献
Wagenaar, Anno; Kirby, Anthony J.; Engberts, Jan B. F. N.
Recueil des Travaux Chimiques des Pays-Bas, 1985 , vol. 104, # 7-8 p. 203 - 205
反应条件
potassium permanganate
参考文献
Bl.Nagoya City Univ.pharm.SchoolChem.Abstr., , vol. 2, p. 42
Bl.Nagoya City Univ.pharm.SchoolChem.Abstr., , p. 11280
反应条件
In(OSO2CF3)3 in 1,2-dichloro-ethane
T=100°C; 24 h;
参考文献
Syngenta Limited, Syngenta Limited
Patent: WO2004/31134 A1, 2004 ;
Location in patent: Page 5;6 ;
反应条件
sodium iodide in dimethyl sulfoxide
T=20°C; Electrochemical reaction;
参考文献
Huang, Haolai; Yuan, Gaoqing; Li, Xianwei; Jiang, Huanfeng
Tetrahedron Letters, 2013 , vol. 54, # 52 p. 7156 - 7159
反应条件
triethylamine in dichloromethane
T=0 - 20°C; 1 h;
参考文献
TOYAMA CHEMICAL CO., LTD.; Hirono, Shuichi; Shiozawa, Shunichi
Patent: EP1445249 A1, 2004 ;
Location in patent: Page 134 ;
反应条件
potassium carbonate in acetonitrile
T=20°C; 17 h;
参考文献
S*BIO PTE LTD
Patent: WO2005/40101 A1, 2005 ;
Location in patent: Page/Page column 60-61 ;
参考文献
Fischer, Walter; Grob, Cyril A.; Sprecher, Georg von; Waldner, Adrian
Helvetica Chimica Acta, 1980 , vol. 63, # 4 p. 928 - 937
反应条件
sodium hypochlorite in water
Ambient temperature;
参考文献
Tang, Xiaodong; Huang, Liangbin; Qi, Chaorong; Wu, Xia; Wu, Wanqing; Jiang, Huanfeng
Chemical Communications, 2013 , vol. 49, # 54 p. 6102 - 6104
反应条件
dimethyl amine in tetrahydrofuran
参考文献
Imperial Chemical Industries PLC; ICI Pharma
Patent: US5314891 A1, 1994 ;
US 5314891 A
反应条件
1: With 2,4,6-trichloro-1,3,5-triazine in acetonitrile
T=20°C; 0.5 h;
2: With triethylamine in acetonitrile
参考文献
Rad, Mohammad Navid Soltani; Khalafi-Nezhad, Ali; Asrari, Zeinab; Behrouz, Somayeh; Amini, Zohreh; Behrouz, Marzieh
Synthesis, 2009 , # 23 art. no. Z15009SS, p. 3983 - 3988
