2-(1,2-苯异噁唑-3-基)乙酸甲酯合成路线 (共 17 条)
反应条件
hydrogenchloride in methanol
反应条件
sodium methylate in methanol 2 h;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1013 - 1022
反应条件
sodium methylate in methanol 4 h;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1013 - 1022
反应条件
1: 76 percent / conc. sulphuric acid / 20 h / Heating 2: 70 percent / sodium metaperiodate / H2O; methanol / 18 h / 50 °C 3: 84 percent / NaOH / 5 h / other reagent View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1013 - 1022
反应条件
1: 73 percent / conc. sulphuric acid / 15 h / Heating 2: 65 percent / m-chloroperbenzoic acid / CHCl3 / 1 h / Ambient temperature 3: 86 percent / MeONa / 2 h / other reagent View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1013 - 1022
反应条件
in methanol; diethyl ether T=0 - 20°C;
参考文献
Fallan, Charlene; Lam, Hon Wai
Chemistry - A European Journal, 2012 , vol. 18, # 36 p. 11214 - 11218
反应条件
1: 70 percent / sodium metaperiodate / H2O; methanol / 18 h / 50 °C 2: 84 percent / NaOH / 5 h / other reagent View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1013 - 1022
反应条件
1: 65 percent / m-chloroperbenzoic acid / CHCl3 / 1 h / Ambient temperature 2: 86 percent / MeONa / 2 h / other reagent View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1013 - 1022
反应条件
1: 0.52 g / NaH / tetrahydrofuran / 1 h / 0 °C 2: 71 percent / 2.5 h View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1013 - 1022
反应条件
sulfuric acid 1.5 h; Heating;
参考文献
Journal of Medicinal Chemistry, , vol. 46, # 25 p. 5428 - 5436