4,5-二甲氧基-2-(2-丙烯基)苯酚合成路线 （共 10 条）
反应条件
in neat (no solvent)
T=235 - 240°C; 0.75 h;
参考文献
Buechi, George; Chu, Ping-Sun
Journal of the American Chemical Society, 1981 , vol. 103, # 10 p. 2718 - 2721
反应条件
1: K2CO3 / acetone
2: 240 °C
View Scheme
参考文献
Van Otterlo, Willem A.L.; Ngidi, E. Lindani; Coyanis, E. Mabel; De Koning, Charles B.
Tetrahedron Letters, 2003 , vol. 44, # 2 p. 311 - 313
反应条件
decalin
T=220°C; Claisen rearrangement; 12 h;
参考文献
Argueelles, Nancy; Sanchez-Sandoval, Eugenia; Mendieta, Aaron; Villa-Tanaca, Lourdes; Garduno-Siciliano, Leticia; Jimenez, Fabiola; Cruz, Maria del Carmen; Medina-Franco, Jose L.; Chamorro-Cevallos, German; Tamariz, Joaquin
Bioorganic and Medicinal Chemistry, 2010 , vol. 18, # 12 p. 4238 - 4248
反应条件
1: potassium carbonate; acetone
2: aqueous KOH-solution
View Scheme
参考文献
Arnold; Bortnick
Journal of the American Chemical Society, 1945 , vol. 67, p. 806
反应条件
1: aqueous KOH-solution
View Scheme
参考文献
Arnold; Bortnick
Journal of the American Chemical Society, 1945 , vol. 67, p. 806
反应条件
Claisen rearrangement;
参考文献
Cartus, Alexander T.; Merz, Karl-Heinz; Schrenk, Dieter
Drug Metabolism and Disposition, 2011 , vol. 39, # 9 p. 1727 - 1733
反应条件
Erhitzen auf Siedetemperatur;
参考文献
Arnold; Bortnick
Journal of the American Chemical Society, 1945 , vol. 67, p. 806
反应条件
5 Pd(II)/C(eggshell); hydrogen in ethanol
T=20°C; P=1034.32 Torr; 12 h;
参考文献
Argueelles, Nancy; Sanchez-Sandoval, Eugenia; Mendieta, Aaron; Villa-Tanaca, Lourdes; Garduno-Siciliano, Leticia; Jimenez, Fabiola; Cruz, Maria del Carmen; Medina-Franco, Jose L.; Chamorro-Cevallos, German; Tamariz, Joaquin
Bioorganic and Medicinal Chemistry, 2010 , vol. 18, # 12 p. 4238 - 4248
反应条件
lithium perchlorate in methanol
anodic oxidation;
参考文献
Shizuri, Yoshikazu; Yamamura, Shosuke
Tetrahedron Letters, 1983 , vol. 24, # 45 p. 5011 - 5012
反应条件
2,3-dicyano-5,6-dichloro-p-benzoquinone
0.75 h; Ambient temperature; Yield given;
参考文献
Angle, Steven R.; Turnbull, Kenneth D.
Journal of Organic Chemistry, 1993 , vol. 58, # 20 p. 5360 - 5369
