对硝基苯基 2,3,4,6-O-四乙酰基-beta-D-吡喃葡萄糖苷合成路线 (共 27 条)
反应条件
silver imidazolate; 3 A molecular sieve; zinc(II) chloride in dichloromethane T=40°C; 48 h;
参考文献
Patil, Premanand Ramrao; Ravindranathan Kartha
Journal of Carbohydrate Chemistry, 2008 , vol. 27, # 7 p. 411 - 419
反应条件
1: in dichloromethane T=0°C; Molecular sieveInert atmosphere; 2: With boron trifluoride diethyl etherate in dichloromethane 3 h; Molecular sieveInert atmosphere;
参考文献
Li, Yali; Mo, Huaping; Lian, Gaoyan; Yu, Biao
Carbohydrate Research, 2012 , vol. 363, p. 14 - 22
反应条件
pyridine 5 h; cooling;
参考文献
Kawano, Shin-Ichiro; Tamaru, Shun-Ichi; Fujita, Norifumi; Shinkai, Seiji
Chemistry - A European Journal, 2004 , vol. 10, # 2 p. 343 - 351
反应条件
Ag(1+)*C14H24AgN4O2(1+)*2Cl(1-) in acetonitrile T=25°C; 3 h; Darkness; stereoselective reaction;
参考文献
Talisman, Ian J.; Kumar, Vineet; Deschamps, Jeffrey R.; Frisch, Mark; Malhotra, Sanjay V.
Carbohydrate Research, 2011 , vol. 346, # 15 p. 2337 - 2341
反应条件
boron trifluoride diethyl etherate; triethylamine in dichloromethane 41 h;
参考文献
Lee, Yeon Soo; Rho, Eun Suk; Min, Yong Ki; Kim, Bum Tae; Kim, Ki Ho
Journal of Carbohydrate Chemistry, 2001 , vol. 20, # 6 p. 503 - 506
反应条件
trimethylsilyl trifluoromethanesulfonate in dichloromethane T=-20°C; 0.833333 h;
参考文献
Li; Cai
Synthetic Communications, 1992 , vol. 22, # 14 p. 2121 - 2124
反应条件
copper(II) sulfate T=130°C; 0.25 h;
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 19, # 9 p. 825 - 826
反应条件
boron trifluoride diethyl etherate; N,N,N',N'-tetramethylguanidine in acetonitrile 3 h; Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 4 p. 1079 - 1082
反应条件
1: 98 percent / BiBr3; Me3SiBr / CH2Cl2 / 20 °C 2: 70 percent / Ag2O / acetonitrile / 1 h / Heating View Scheme
参考文献
Farmaco, , vol. 56, # 4 p. 319 - 324
参考文献
Journal of Experimental Medicine, , vol. 50, p. 521,528