1,3-二氢异苯并呋喃-1-醇合成路线 (共 15 条)
反应条件
manganese(IV) oxide in tetrahydrofuran T=45°C; Rate constant;
参考文献
Constantinides, Ioannis; Macomber, Roger S.
Journal of Organic Chemistry, 1992 , vol. 57, # 22 p. 6063 - 6067
反应条件
diisobutylaluminium hydride in hexane; dichloromethane
T=-78°C; 1.5 h;
参考文献
Mikami, Koichi; Ohmura, Hirofumi
Organic Letters, 2002 , vol. 4, # 20 p. 3355 - 3357
反应条件
tri-n-butyl-tin hydride; tetrakis(triphenylphosphine) palladium(0) in toluene
T=50°C; P=760 Torr; Yields of byproduct given;
参考文献
Baillargeon, Victor P.; Stille, J. K.
Journal of the American Chemical Society, 1983 , vol. 105, # 24 p. 7175 - 7176
反应条件
1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione in dimethyl sulfoxide
T=23°C; 23 h;
参考文献
Corey, E. J.; Palani, Anandan
Tetrahedron Letters, 1995 , vol. 36, # 20 p. 3485 - 3488
反应条件
1: With 2-hydroxy-1,3-isoindolinedione; 2,2'-azo-bisisobutyronitrile; oxygen in acetonitrile
T=75°C; P=760.051 Torr; 20 h;
2: With triphenylphosphine in acetonitrile
T=25°C; Further stages.;
参考文献
Fukuda, Osamu; Sakaguchi, Satoshi; Ishii, Yasutaka
Advanced Synthesis and Catalysis, 2001 , vol. 343, # 8 p. 809 - 813
反应条件
3,3-dimethyldioxirane in dichloromethane; acetone
0.166667 h; Ambient temperature;
参考文献
Bovicelli, Paolo; Sanetti, Anna; Bernini, Roberta; Lupattelli, Paolo
Tetrahedron, 1997 , vol. 53, # 28 p. 9755 - 9760
参考文献
Daicel Chemical Industries, Ltd.
Patent: US6201156 B1, 2001 ;
反应条件
Co(acetylacetonate)3; oxygen in ethyl acetate
T=70°C; 24 h;
参考文献
Reetz, Manfred T.; Toellner, Karl
Tetrahedron Letters, 1995 , vol. 36, # 52 p. 9461 - 9464
反应条件
manganese(IV) oxide in dichloromethane
1 h; Ambient temperature;
参考文献
Endo, Katsuya; Takahashi, Hiroyasu; Aihara, Minako
Heterocycles, 1996 , vol. 42, # 2 p. 589 - 615