2-氯-2-丙烯-1-醇合成路线 （共 34 条）
参考文献
Bristow
Transactions of the Faraday Society, 1958 , vol. 54, p. 1064
反应条件
n-butyllithium; bis(1,3-diphenylphosphinopropane) nickel(II) chloride
1.) THF, hexane, 0 deg C, 10 min, 2.) reflux, 3 h; Yield given. Multistep reaction;
参考文献
Organ, Michael G.; Murray, Aaron P.
Journal of Organic Chemistry, 1997 , vol. 62, # 5 p. 1523 - 1526
参考文献
Le Baut; Sparfel; Clairc; et al.
European Journal of Medicinal Chemistry, 1983 , vol. 18, # 5 p. 441 - 445
反应条件
thionyl chloride in diethyl ether
3 h; Heating;
参考文献
Le Baut; Sparfel; Clairc; et al.
European Journal of Medicinal Chemistry, 1983 , vol. 18, # 5 p. 457 - 463
反应条件
triethylamine in diethyl ether
T=20°C; Acetylation; 1 h;
参考文献
Kadota, Joji; Komori, Shinji; Fukumoto, Yoshiya; Murai, Shinji
Journal of Organic Chemistry, 1999 , vol. 64, # 20 p. 7523 - 7527
反应条件
chlorosulfonic acid
T=96 - 108°C;
参考文献
Dow Chem.Co.
Patent: US2127660 , 1937 ;
反应条件
n-butyllithium; bis(1,3-diphenylphosphinopropane) nickel(II) chloride
1.) THF, hexane, 0 deg C, 10 min, 2.) reflux, 3 h; Yield given. Multistep reaction;
参考文献
Organ, Michael G.; Murray, Aaron P.
Journal of Organic Chemistry, 1997 , vol. 62, # 5 p. 1523 - 1526
反应条件
pyridine; phosphorus tribromide
参考文献
Kremer
Bulletin de la Societe Chimique de France, 1948 , p. 166
反应条件
sulfuric acid; benzene
unter Abdestillieren des Reaktionswassers;
参考文献
Rehberg; Fisher
Patent: US2464992 , 1946 ;
Full Text Show Details
Rehberg; Fisher
Patent: US2410551 , 1944 ;
Full Text Show Details
Rehberg; Fisher
Journal of Organic Chemistry, 1947 , vol. 12, p. 226,227
Chem.Abstr., 1949 , p. 4686
反应条件
toluene-4-sulfonic acid
unter Abdestillieren des Reaktionswassers;
参考文献
Rehberg; Fisher
Patent: US2388440 , 1943 ;
