2,2-二甲基-3-羟基丙醛合成路线 (共 61 条)
反应条件
acetic acid T=35°C; 8 h;
参考文献
Jin, Yong-Sheng; Zhang, Wei; Zhang, Da-Zhi; Qiao, Li-Ming; Wu, Qiu-Ye; Chen, Hai-Sheng
Asian Journal of Chemistry, 2011 , vol. 23, # 3 p. 1117 - 1119
反应条件
1 Au-Pd/TiO2; oxygen; sodium hydroxide T=80°C; P=2250.23 Torr; 4 h;
参考文献
Catalysis Letters, , vol. 142, # 9 p. 1114 - 1120
反应条件
triethylamine in water Aldol Condensation; Product distribution / selectivity;
参考文献
US2007/32682 A1, ;
Page/Page column 4; 6; 7 ;
反应条件
1: benzene 2: aq. H2SO4 View Scheme
参考文献
Chemische Berichte, , vol. 105, p. 1350 - 1355
反应条件
hydrogen; Pd-BaSO4 1) water, 15 min, pH 7.7 2) pH 1.7; Multistep reaction. Title compound not separated from byproducts;
参考文献
Carbohydrate Research, , vol. 210, p. 21 - 38
反应条件
triethylamine T=0 - 65°C; 6 h; Inert atmosphereReflux; Optical yield = 16 percent de; diastereoselective reaction;
参考文献
Toermaekangas, Olli P.; Saarenketo, Pauli; Koskinen, Ari M. P.
Organic Process Research and Development, 2002 , vol. 6, # 2 p. 125 - 131
反应条件
1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione in dimethylsulfoxide-d6 T=23°C; product ratio was determined by 1H NMR; Product distribution;
参考文献
Tetrahedron Letters, , vol. 36, # 44 p. 7945 - 7948
参考文献
Journal of the American Chemical Society, , vol. 134, # 3 p. 1474 - 1477
参考文献
Monatshefte fuer Chemie, , vol. 23, p. 469
参考文献
Monatshefte fuer Chemie, , vol. 23, p. 469