(二甲基胺基)磷酸二甲酯合成路线 (共 12 条)
反应条件
further reagent: FSO3H; KineticsMechanism;
参考文献
Modro, Tomasz A.
Journal of the Chemical Society, Chemical Communications, 1980 , # 5 p. 201 - 202
反应条件
NaOD in water-d2 T=25°C; relative reactivity of the P-O and P-N bond; Rate constant;
参考文献
Davidowitz, Bette; Modro, Tomasz A.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1985 , p. 303 - 306
反应条件
1: phosphonic acid dimethyl ester With 1,3-Dichloro-5,5-dimethyl-2,4-imidazolidinedione in acetonitrile
2: dimethyl amine With cesium fluoride
T=25°C; 0.333333 h;
参考文献
Gupta, Arvind K.; Dubey, Devendra K.; Kaushik
Phosphorus, Sulfur and Silicon and the Related Elements, 2008 , vol. 183, # 7 p. 1641 - 1658
参考文献
Davidowitz, Bette; Modro, Tomasz A.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1985 , p. 303 - 306
反应条件
(i) PCl3, quinoline, Et2O, (ii) N-chloro-succinimide, benzene, (iii) /BRN= 605257/; Multistep reaction;
参考文献
Oeney,I.; Caplow,M.
Journal of the American Chemical Society, 1967 , vol. 89, p. 6972 - 6980
参考文献
Symes, Jill; Modro, Tomasz A.
Canadian Journal of Chemistry, 1986 , vol. 64, p. 1702 - 1708
反应条件
tetrachloromethane; benzene
参考文献
Kamai; Charrasowa
Zhurnal Obshchei Khimii, 1957 , vol. 27, p. 3064;engl.Ausg.S.3093
参考文献
Cheymol et al.
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1959 , vol. 249, p. 1240
反应条件
in toluene
0.25 h; Ambient temperaturefurther benzothiazol-2-yl sulphenamides, further phosphite (substituent effect); Mechanism;
参考文献
Brownbridge, P.; Jowett, I. C.
Phosphorus and Sulfur and the Related Elements, 1988 , vol. 35, p. 311 - 318
参考文献
Schrader
Ang. Ch. Monogr., 1952 , vol. 62, p. 10,11
Full Text Show Details
Kovache et al.
Chimie et Industrie (Paris), 1950 , vol. 64, p. 287,290