N-甲基-4-氨基苯甲醚合成路线 （共 125 条）
反应条件
1.1: sodium hydride / tetrahydrofuran / 0.5 h / 0 °C / |Inert atmosphere 1.2: 0 - 20 °C / |Inert atmosphere 2.1: hydrogenchloride / water; ethylene glycol / 24 h / |Reflux; |Inert atmosphere View Scheme
参考文献
Organic and Biomolecular Chemistry, , vol. 10, # 43 p. 8692 - 8700
反应条件
1: 100 percent / CH2Cl2 / 0.17 h / 20 °C 2: 93 percent / 1,8-diazabicyclo[5.4.0]undec-7-ene / acetonitrile / 20 °C View Scheme
参考文献
Tetrahedron, , vol. 62, # 25 p. 6100 - 6106
反应条件
1: 83 percent / benzene / 8 h / Heating 2: 71 percent / aqueous Sodium Hydroxide / 1 h / Heating View Scheme
参考文献
Synthesis, , # 4 p. 295 - 296
反应条件
Product distribution / selectivity;
参考文献
Obshestvo S Ogranichennoy Otvetstvennostiu Inoxim; Company IFO, LLC; Ivanov, Youri Alexandrovich; Frolov, Alexander Yourievich; Osinin, Valeriy Vladimirovich; Perevezentzev, Vladimir Mixaylovich
Patent: EP2014643 A1, 2009 ;
Location in patent: Page/Page column 7 ;
反应条件
Basolite® A100 T=170°C; 8 h;
参考文献
Applied Catalysis A: General, , vol. 378, # 1 p. 19 - 25
反应条件
sulfuric acid T=150°C;
参考文献
Chemische Berichte, , vol. 54, p. 1665 Anm.1
反应条件
hydrogenchloride; thiourea in ethanol T=25°C; investigation effect of substituents on the rate constant for denitrosation under different conditions; determined by UV spectroscopy; Rate constant;
参考文献
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), , # 11 p. 1803 - 1808
反应条件
lithium aluminium tetrahydride; palladium on activated charcoal 1) THF, 20 min, -30 deg C, 2) 20 deg C, 2 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Tetrahedron, , vol. 43, # 18 p. 4221 - 4226
反应条件
(ethyl)-triphenylphosphonium iodide T=170°C; 0.75 h; Further byproducts given;
参考文献
Journal of Organic Chemistry, , vol. 71, # 15 p. 5770 - 5773
反应条件
sodium tetrahydroborate in dimethyl sulfoxide
参考文献
Journal of Organic Chemistry, , vol. 75, # 5 p. 1378 - 1385
