3-(4-甲氧基苯基)吡啶合成路线 （共 64 条）
反应条件
potassium carbonate; cyclopallated ferrocenylimine c in water; N,N-dimethyl-formamide
T=110°C; Suzuki cross-coupling reaction; 6 h;
参考文献
Zhang, Jinli; Zhao, Liang; Song, Maoping; Mak, Thomas C.W.; Wu, Yangjie
Journal of Organometallic Chemistry, 2006 , vol. 691, # 6 p. 1301 - 1306
反应条件
potassium carbonate; cyclopallated ferrocenylimine c in water; N,N-dimethyl-formamide
T=110°C; Suzuki cross-coupling reaction; 10 h;
参考文献
Zhang, Jinli; Zhao, Liang; Song, Maoping; Mak, Thomas C.W.; Wu, Yangjie
Journal of Organometallic Chemistry, 2006 , vol. 691, # 6 p. 1301 - 1306
反应条件
bis(η3-allyl-μ-chloropalladium(II)); 1,4-di(diphenylphosphino)-butane; potassium hydroxide in water; tert-butyl alcohol
T=90°C;
参考文献
Boehner, Christine M.; Frye, Elizabeth C.; O'Connell, Kieron M. G.; Galloway, Warren R. J. D.; Sore, Hannah F.; Dominguez, Patricia Garcia; Norton, David; Hulcoop, David G.; Owen, Martin; Turner, Gillian; Crawford, Claire; Horsley, Helen; Spring, David R.
Chemistry - A European Journal, 2011 , vol. 17, # 47 p. 13230 - 13239
反应条件
tetrakis(triphenylphosphine) palladium(0); sodium carbonate in 1,4-dioxane
Suzuki cross-coupling reaction; 16 h; Heating;
参考文献
Cioffi, Christopher L.; Spencer, William T.; Richards, Justin J.; Herr, R. Jason
Journal of Organic Chemistry, 2004 , vol. 69, # 6 p. 2210 - 2212
反应条件
palladium diacetate
T=100°C; Stille cross-coupling; 15 h; Ionic liquid;
参考文献
Louaisil, Nicolas; Pham, Phuoc Dien; Boeda, Fabien; Faye, Djibril; Castanet, Anne-Sophie; Legoupy, Stephanie
European Journal of Organic Chemistry, 2011 , # 1 p. 143 - 149
反应条件
potassium hydroxide; tetrakis(triphenylphosphine) palladium(0); tetrabutylammomium bromide in tetrahydrofuran
3 h; Heating;
参考文献
Ishikura, Minoru; Kamada, Machiko; Terashima, Masanao
Heterocycles, 1984 , vol. 22, # 2 p. 265 - 268
反应条件
Cp2Ni; potassium tert-butylate; triphenylphosphine
T=100°C; 12 h; Inert atmosphere;
参考文献
Kobayashi, Osamu; Uraguchi, Daisuke; Yamakawa, Tetsu
Organic Letters, 2009 , vol. 11, # 12 p. 2679 - 2682
反应条件
1.1: 73 percent / diethyl ether / 0 - 20 °C
2.1: TBAF / tetrahydrofuran
2.2: 71 percent / TBAF; (t-Bu)3P / [(allyl)PdCl]2 / tetrahydrofuran / 5 h / Heating
View Scheme
参考文献
Denmark, Scott E.; Wu, Zhicai
Organic Letters, 1999 , vol. 1, # 9 p. 1495 - 1498
反应条件
potassium tert-butylate
T=110°C; 8 h;
参考文献
Bhakuni, Bhagat Singh; Yadav, Abhimanyu; Kumar, Shailesh; Kumar, Sangit
New Journal of Chemistry, 2014 , vol. 38, # 2 p. 827 - 836
反应条件
1: 97 percent / Mg / tetrahydrofuran / 12 h / Ambient temperature
2: 69 percent / KF / Pd(OAc)2, P(o-Tol)3 / dimethylformamide / 120 °C
View Scheme
参考文献
Hatanaka, Yasuo; Goda, Ken-ichi; Okahara, Yoshinori; Hiyama, Tamejiro
Tetrahedron, 1994 , vol. 50, # 28 p. 8301 - 8316
