1: in diethyl ether; benzene T=0 - 20°C; 2 h; Inert atmosphere; 2: With water; ammonium chloride in diethyl ether; benzene Inert atmosphere;

1: 2-bromo-4-methyl-pyridine With n-butyllithium in diethyl ether; hexane T=-78°C; 0.166667 - 0.5 h; 2: N,N-dimethyl acetamide in diethyl ether; hexane T=20°C; 2 - 14.5 h; Product distribution / selectivity;

tert.-butylhydroperoxide; iron(II) sulfate; trifluoroacetic acid in acetonitrile 4 h; Heating;

暂无反应条件数据

1: 30 percent / silver nitrate, ammonium persulfate, conc. H2SO4 / H2O; CH2Cl2 / 3 h / 40 °C 2: benzene; 2-methyl-propan-2-ol / 5 h / Irradiation View Scheme

1: diazonium reaction View Scheme

ammonium acetate; sodium hydroxide; acetic acid in tetrahydrofuran; toluene

1.1: sodium acetate / dimethyl sulfoxide / 20 - 25 °C 2.1: potassium carbonate; methanol / 1 h / 20 °C 3.1: sodium hydride / tetrahydrofuran; mineral oil / 1.32 h / 0 - 40 °C 3.2: 20 - 40 °C 4.1: cyclohexane; hexane / 3.25 h / 10 - 20 °C 5.1: lithium diisopropyl amide / tetrahydrofuran / 1 h / -15 °C 5.2: 1.5 h / -15 °C 5.3: 0.42 h / 10 - 20 °C / pH 2 - 4 6.1: N-bromosuccinmide / toluene; ethanol / 1.5 h / 40 °C 7.1: pyridine / tetrahydrofuran / 1.5 h / 40 °C 8.1: water; tetrahydrofuran / 2.5 h / 60 °C View Scheme