(2-丙烯基)膦酸二乙酯合成路线 (共 11 条)
反应条件
hydrogenchloride; water; oxygen; palladium dichloride T=85°C; 20 h;
参考文献
Sturtz, Georges; Pondaven-Raphalen, Annick
Journal of Chemical Research, Miniprint, 1980 , # 5 p. 2512 - 2523
反应条件
in tetrahydrofuran; hexane T=-78°C; 0.166667 h; Yield given. Yields of byproduct given;
参考文献
Bulletin de la Societe Chimique de France, , vol. 130, p. 668 - 672
反应条件
Grubb's 2nd generation catalyst; polydimethylsiloxane in methanol; water
T=50°C; 20 h;
参考文献
Brett Runge; Mwangi, Martin T.; Bowden, Ned B.
Journal of Organometallic Chemistry, 2006 , vol. 691, # 24-25 p. 5278 - 5288
反应条件
dihydrogen peroxide in pyridine
Ambient temperature;
参考文献
Mikolajczyk, Marian; Grzejszczak, Slawomir; Korbacz, Katarzyna
Tetrahedron Letters, 1981 , vol. 22, # 32 p. 3097 - 3100
反应条件
amberlyst-15 resin
T=20°C; 0.383333 h; neat (no solvent);
参考文献
Kunda, U.M. Rao; Mudumala, V.N. Reddy; Reddy Gangireddy; Nemallapudi; Sandip; Cirandur
Chinese Chemical Letters, 2011 , vol. 22, # 8 p. 895 - 898
反应条件
1: 1.) Se, n-BuLi
2: 80 percent / H2O2 / pyridine / Ambient temperature
View Scheme
参考文献
Mikolajczyk, Marian; Grzejszczak, Slawomir; Korbacz, Katarzyna
Tetrahedron Letters, 1981 , vol. 22, # 32 p. 3097 - 3100
反应条件
triethylamine in benzene
参考文献
Pudovik,A.N. et al.
Doklady Chemistry, 1965 , vol. 165, # 3 p. 1132 - 1134
Doklady Akademii Nauk SSSR, 1965 , vol. 165, # 3 p. 586 - 589
反应条件
in neat (no solvent)
T=60 - 100°C;
参考文献
Gaydou,E.M.
Bulletin de la Societe Chimique de France, 1973 , p. 2275 - 2278
反应条件
phosphorus; phosphorus pentachloride; trimethylamine; phenol
Yield given. Multistep reaction;
参考文献
Ivanov, B. E.; Fridland, N. S.; Abul'khanov, A. G.; Krokhina, S. S.; Il'yasov, A. V.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1987 , vol. 36, # 6 p. 1293 - 1296
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1987 , vol. 36, # 6 p. 1399 - 1402
参考文献
Teulade, Marie-Paule; Savignac, Philippe; Aboujaoude, Elie Elia; Collignon, Noel
Journal of Organometallic Chemistry, 1986 , vol. 312, p. 283 - 296