(3E)-1,6-二溴-3-己烯合成路线 （共 10 条）
反应条件
2: H2 / PtO2 View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 6, p. 402 - 405
反应条件
carbon tetrabromide; triphenylphosphine in dichloromethane
15 h;
参考文献
McNaughton, Brian R.; Bucholtz, Kevin M.; Camaano-Moure, Ana; Miller, Benjamin L.
Organic Letters, 2005 , vol. 7, # 4 p. 733 - 736
反应条件
Grubb's 2nd generation catalyst; ethene in dichloromethane
T=20°C; P=760.051 Torr; 48 h;
参考文献
Vaswanl, Rishi G.; Day, Joshua J.; Wood, John L.
Organic Letters, 2009 , vol. 11, # 20 p. 4532 - 4535
反应条件
1: 85 percent / H+
2: 82 percent / LiAlH4
3: 85 percent / CBr4, triphenylphosphine
View Scheme
参考文献
Gassman, Paul G.; Mlinaric-Majerski, Kata
Journal of Organic Chemistry, 1986 , vol. 51, # 12 p. 2397 - 2398
反应条件
1: 82 percent / LiAlH4
2: 85 percent / CBr4, triphenylphosphine
View Scheme
参考文献
Gassman, Paul G.; Mlinaric-Majerski, Kata
Journal of Organic Chemistry, 1986 , vol. 51, # 12 p. 2397 - 2398
反应条件
Mo(CHCMe2Ph)lt;N-2,6-(i-Pr)2C6H3gt;lt;OCMe(CF3)2gt;2 in dichloromethane
3 h; Ambient temperature;
参考文献
Crowe, William E.; Goldberg, Daniel R.
Journal of the American Chemical Society, 1995 , vol. 117, # 18 p. 5162 - 5163
反应条件
Mo(CHCMe2Ph)(NAr)lt;OCMe(CF3)2gt;2 (Schrock's molybdenum catalyst) in ethylene glycol dimethyl ether
4 h; Yields of byproduct given;
参考文献
Crowe, William E.; Goldberg, Daniel R.; Zhang, Zhijia J.
Tetrahedron Letters, 1996 , vol. 37, # 13 p. 2117 - 2120
反应条件
1: lithium alanate; diethyl ether
2: pyridine; phosphorus (III)-bromide
View Scheme
参考文献
Lukes; Dudek
Collection of Czechoslovak Chemical Communications, 1959 , vol. 24, p. 2484,2489
反应条件
1: HCl
2: LiAlH4
3: PBr3, Py
View Scheme
参考文献
Burger,A.; Bedford,G.R.
Journal of Medicinal Chemistry, 1963 , vol. 6, p. 402 - 405
参考文献
Myrsina,R.A.; Kuznetsov,N.V.
Sov. Prog. Chem. (Engl. Transl.), 1976 , vol. 42, # 4 p. 407 - 410,70 - 73
