N-叔丁氧羰基-L-丝氨酸合成路线 (共 19 条)
参考文献
Stocking, Emily M.; Schwarz, Jessie N.; Senn, Hans; Salzmann, Michael; Silks, Louis A.
Journal of the Chemical Society - Perkin Transactions 1, 1997 , # 16 p. 2443 - 2447
反应条件
caesium carbonate in N,N-dimethyl-formamide T=20°C; 12 h;
参考文献
UNIVERSITY OF VIRGINIA PATENT FOUNDATION
Patent: WO2005/41899 A2, 2005 ;
Location in patent: Page/Page column 94; 102-103 ;
WO 2005/041899 A2
反应条件
triethylamine in α,α,α-trifluorotoluene T=120°C; 0.333333 h; Microwave irradiation;
参考文献
Wang, Teng-Wei; Intaranukulkit, Tanit; Rosana, Michael R.; Slegeris, Rimantas; Simon, Janet; Dudley, Gregory B.
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 2 p. 248 - 250
反应条件
triethylamine in dichloromethane 2 h;
参考文献
Sowinski, Jennifer A.; Toogood, Peter L.
Journal of Organic Chemistry, 1996 , vol. 61, # 22 p. 7671 - 7676
反应条件
1: Me2NP(NMe2)(=NEt)N=P(NMe2)3 / acetonitrile / 16 h / 20 °C 2: acetonitrile / 6 h / 20 °C View Scheme
参考文献
Organic letters, , vol. 4, # 23 p. 4005 - 4008
反应条件
potassium carbonate in dichloromethane 8 h; Ambient temperature;
参考文献
Nakata, Takashi; Nakatani, Masaru; Takahashi, Masatoshi; Okai, Jiro; Kawaoka, Yoshiaki; Kouge, Katsushige; Okai, Hideo
Bulletin of the Chemical Society of Japan, 1996 , vol. 69, # 4 p. 1099 - 1106
反应条件
1: benzyl alcohol With copper(II) bis(trifluoromethanesulfonate); (4-cyclohexyl-2,4-diazabuta-2,3-dienyl)polystyrene resin in tetrahydrofuran T=20°C; 16 h; 2: With N,N,N',N,-tetramethylethylenediamine in N,N-dimethyl-formamide 3: t-butyloxycarbonyl-L-serine in tetrahydrofuran T=60°C; 16 h;
参考文献
Organic Letters, , vol. 5, # 6 p. 853 - 856
反应条件
in dimethyl sulfoxide; Petroleum ether
反应条件
1: 74 percent / CCl4 / 8 h / Heating 2: 81 percent / 1 M NaOH / tetrahydrofuran / 1 h / Ambient temperature View Scheme
参考文献
Journal of Organic Chemistry, , vol. 57, # 12 p. 3397 - 3404
参考文献
Gajewski, Mariusz; Seaver, Ben; Esslinger, C. Sean
Bioorganic and Medicinal Chemistry Letters, 2007 , vol. 17, # 15 p. 4163 - 4166