(2Rs)-2-[4-(2-甲基丙基)苯基]丙酰胺合成路线 (共 5 条)
反应条件
ammonium hydroxide 4 h; Ambient temperature;
参考文献
Valenti; Rampa; Fabbri; Giusti; Cima
Archiv der Pharmazie, 1983 , vol. 316, # 9 p. 752 - 755
反应条件
[Ru(η6-C6Me6)Cl2(tris(dimethylamino)phosphine)]; water T=150°C; 1 h; Inert atmosphereMicrowave irradiation;
参考文献
Garcia-Alvarez, Rocio; Diez, Josefina; Crochet, Pascale; Cadierno, Victorio
Organometallics, 2011 , vol. 30, # 20 p. 5442 - 5451
反应条件
1: oxalyl chloride, DMF / CH2Cl2 / 8 h / Ambient temperature 2: conc. aq. NH3 / CH2Cl2 / 1 h View Scheme
参考文献
Bioorganic and Medicinal Chemistry, , vol. 5, # 2 p. 393 - 396
反应条件
tetraethylammonium bromide; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione in acetonitrile T=20 - 60°C;
参考文献
Bellale, Eknath V.; Bhalerao, Dinesh S.; Akamanchi, Krishnacharya G.
Journal of Organic Chemistry, 2008 , vol. 73, # 23 p. 9473 - 9475
反应条件
phosgene in chloroform; toluene 12 h;
参考文献
DOMPE S.P.A.
Patent: WO2005/28425 A2, 2005 ;
Location in patent: Page/Page column 11 ;