反应条件
in tetrachloromethane dropwise addn. of dimethylsulfoxide (15.4mmol) to refluxing suspension of (CH3)3SnN(SO2CH3) in CCl4 (50ml), formation of a clear soln:; formation of crystals after 3d, -15°C; idenification of tetramethyl tin by GC-MS coupling;;
参考文献
Blaschette, Armand; Hippel, Ilona; Krahl, Juergen; Wieland, Elke; Jones, Peter G.; Sebald, Angelika
Journal of Organometallic Chemistry, 1992 , vol. 437, # 3 p. 279 - 297
