反应条件
methyllithium in tetrahydrofuran; diethyl ether under N2 or Ar, dropwise addn. of MeLi in THF/Et2O to Si(SnMe3)4 in THF , stirred for 22 h; removal of volatiles, extn. (pentane), concd., cooled to -40°C, filtered, dried (four crops);
参考文献
Heyn, Richard H.; Tilley, T. Don
Inorganic Chemistry, 1990 , vol. 29, p. 4051 - 4055
