in neat (no solvent)
inert atmosphere; dropwise addn. of 1 equiv. Me4Sb2 to Et2Te2 at 0°C, standing for 1 d; filtration, vac. distn. off of volatiles (bath at 25-30°C); contg. 4percent Et2Te2 as impurity;
参考文献
Dickson, Ron S.; Heazle, Kerryn D.
Journal of Organometallic Chemistry, 1995 , vol. 493, # 1-2 p. 189 - 198
in neat (no solvent, solid phase)
byproducts: HCl; pyrolysis of SbMe3Cl2 at 1043 K, the sample vapour was pyrolysed on passing through a tungsten wire-wrapped molybdenum tube which could be heated by electron bombardment; detd. by mass-spectrometry;
参考文献
Elbel, Susanne; Egsgaard, Helge; Carlsen, Lars
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1987 , p. 481 - 488
Paneth, F.
Transactions of the Faraday Society, 1934 , vol. 30, p. 179
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Paneth, F. A.; Loleit, H.
Journal of the Chemical Society, 1935 , p. 366 - 371
Burg; Grant
Journal of the American Chemical Society, 1959 , vol. 81, p. 1,2,3
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Burg
Inorg.Chem, 1977 , vol. 19, p. 217
