反应条件
carbon monoxide in toluene Placing of a toluene soln. of W-compd. in a pressure bomb under 1100 psi of CO, placing of bomb in oil bath maintained at 112°C for 19 h under 1250 psi.; Cooling, releasing of pressure, quick removal of volatile components in vac., dissolving of mixt. (pentane), column chromy. (Al2O3, pentane), sepn. of resulting compd. by elution with pentane/ether mixt.;
参考文献
Inorganic Chemistry, , vol. 28, p. 2837 - 2846
