3-(氨基磺酰基)噻吩-2-羧酸合成路线 （共 6 条）
反应条件
1: aq. NH3 / acetone / 1 h
2: carbonate buffer / acetonitrile / 29 °C / pH 9.8
View Scheme
参考文献
Bastide; Badon; Cambon; Vega
Pesticide Science, 1994 , vol. 40, # 4 p. 293 - 297
反应条件
1.1: NaNO2; glacial acetic acid; aq. HCl / 1 h / 0 °C
1.2: SO2; CuCl2 / acetic acid / 1 h / 0 °C
2.1: aq. NH3 / acetone / 1 h
3.1: carbonate buffer / acetonitrile / 29 °C / pH 9.8
View Scheme
参考文献
Bastide; Badon; Cambon; Vega
Pesticide Science, 1994 , vol. 40, # 4 p. 293 - 297
反应条件
sodium hydroxide
2 h; Heating;
参考文献
Diaz, Juan A.; Morante, M. Esther; Vega, Salvador; Darias, Victoriano; Abdala, Susana; Delgado, Laura; De Las Heras, Beatriz; Villar, Angel; Vivas, Jose Maria
Archiv der Pharmazie, 1996 , vol. 329, # 5 p. 229 - 238
反应条件
pH 4 buffer; water
T=28°C; var pH; Rate constant;
参考文献
Cambon, Jean-Pierre; Bastide, Jean
Journal of Agricultural and Food Chemistry, 1996 , vol. 44, # 1 p. 333 - 337
反应条件
pH 4 buffer; water
T=28°C; var pH; Rate constant;
参考文献
Cambon, Jean-Pierre; Bastide, Jean
Journal of Agricultural and Food Chemistry, 1996 , vol. 44, # 1 p. 333 - 337
参考文献
BASF Aktiengesellschaft
Patent: US4028373 A1, 1977 ;
