1-(二甲氧基甲基)-3-甲氧基苯合成路线 （共 11 条）
反应条件
chloroacetate buffer; sodium lauryl sulfate in water T=25°C; pH=3.54 - 3.80; Kinetics; Further Variations:ReagentspH-values;
参考文献
Rose, Phillip D. R.; Williams, Andrew
Journal of the Chemical Society, Perkin Transactions 2, 2002 , # 9 p. 1589 - 1595
反应条件
triethylsilane; acetyl chloride; tin(ll) chloride in dichloromethane 3 h; Ambient temperature;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 64, # 4 p. 1410 - 1412
反应条件
triethylsilane; acetyl-bromide; stannous bromide in dichloromethane 2 h; Ambient temperature;
参考文献
Oriyama, Takeshi; Iwanami, Katsuyuki; Tsukamoto, Kazuhisa; Ichimura, Yuichi; Koga, Gen
Bulletin of the Chemical Society of Japan, 1991 , vol. 64, # 4 p. 1410 - 1412
反应条件
triethylsilane; acetyl-bromide; 2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride; stannous bromide 1) CH2CL2, RT, 2.5h, 2) benzene, 0.5h, reflux; also with 2) LiAlH4; Yield given. Multistep reaction;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 64, # 8 p. 2581 - 2582
参考文献
Rose, Phillip D. R.; Williams, Andrew
Journal of the Chemical Society, Perkin Transactions 2, 2002 , # 9 p. 1589 - 1595
反应条件
sodium hydrogencarbonate; trimethyl orthoformate in methanol
参考文献
Tropix, Inc.
Patent: US5225584 A1, 1993 ;
反应条件
1: MnO2 / CH2Cl2 / 20 °C
2: In(OTf)3 / 24 h
View Scheme
参考文献
Smith, Brendan M.; Graham, Andrew E.
Tetrahedron Letters, 2007 , vol. 48, # 28 p. 4891 - 4894
反应条件
ammonium cerium(IV) nitrate; sodium carbonate
0.75 h; Heating;
参考文献
Nair, Vijay; Rajan, Roshini; Balagopal, Lakshmi; Nair, Latha G.; Ros, Sindu; Mohanan, Kishor
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2005 , vol. 44, # 1 p. 141 - 143
反应条件
pyridine-2-carboxylic acid; iron sulphate heptahydrate; dihydrogen peroxide
T=20 - 60°C; 12 h; Schlenk techniqueMolecular sieve;
参考文献
Ray, Ritwika; Chowdhury, Abhishek Dutta; Lahiri, Goutam Kumar
ChemCatChem, 2013 , vol. 5, # 8 p. 2158 - 2161
反应条件
hydrogenchloride
multistep reaction; various catalysts; Product distribution;
参考文献
Bebon-Rampal, C.; Vanhove, D.
Bulletin de la Societe Chimique de France, 1992 , # 5 p. 501 - 508
