2,2,4,4,6,6-六溴联苯合成路线 （共 5 条）
反应条件
1: With lithium diisopropyl amide in tetrahydrofuran; hexane T=-78°C; 2 h; Inert atmosphere; 2: With lithium chloride; copper(I) bromide in hexane T=-78°C; 2 h; Inert atmosphere; 3: With p-benozquinone in tetrahydrofuran; hexane T=-78 - 20°C; 1 h; Inert atmosphere;
参考文献
Graff, Julien; Debande, Thibaut; Praz, Jezabel; Guenee, Laure; Alexakis, Alexandre
Organic Letters, 2013 , vol. 15, # 16 p. 4270 - 4273
反应条件
copper T=200°C; 2 h;
参考文献
Australian Journal of Chemistry, , vol. 38, # 3 p. 391 - 399
反应条件
1: With n-butyllithium in tetrahydrofuran
T=-78°C; 0.166667 h; Inert atmosphere;
2: With methanol in tetrahydrofuran
T=-78 - 20°C; Inert atmosphere;
参考文献
Perron, Quentin; Alexakis, Alexandre
Advanced Synthesis and Catalysis, 2010 , vol. 352, # 14-15 p. 2611 - 2620
反应条件
1: With n-butyllithium in tetrahydrofuran
T=-78°C; 0.166667 h; Inert atmosphere;
2: With methanol in tetrahydrofuran
T=-78 - 20°C; Inert atmosphere;
参考文献
Perron, Quentin; Alexakis, Alexandre
Advanced Synthesis and Catalysis, 2010 , vol. 352, # 14-15 p. 2611 - 2620
反应条件
1: With n-butyllithium in tetrahydrofuran
T=-78°C; 0.166667 h; Inert atmosphere;
2: With methanol in tetrahydrofuran
T=-78 - 20°C; Inert atmosphere;
参考文献
Perron, Quentin; Alexakis, Alexandre
Advanced Synthesis and Catalysis, 2010 , vol. 352, # 14-15 p. 2611 - 2620
