4-乙氧基苯基氨基甲酸叔丁酯合成路线 (共 5 条)
反应条件
1-methylguanidine hydrochloride in ethanol
T=35 - 40°C; 0.1 h;
参考文献
Jahani, Fatemeh; Tajbakhsh, Mahmood; Golchoubian, Hamid; Khaksar, Samad
Tetrahedron Letters, 2011 , vol. 52, # 12 p. 1260 - 1264
反应条件
polymethylhydrosiloxane; palladium on activated charcoal in ethanol
T=20°C; 3 h;
参考文献
Chandrasekhar; Raji Reddy; Jagadeeshwar Rao
Synlett, 2001 , # 10 p. 1561 - 1562
反应条件
polymethylhydrosiloxane; palladium on activated charcoal in ethanol
T=20°C; 5 h;
参考文献
Chandrasekhar; Raji Reddy; Jagadeeshwar Rao
Synlett, 2001 , # 10 p. 1561 - 1562
反应条件
copper (II) 2-ethylhexanoate in benzene
Heating;
参考文献
Francis,T.; Thorne,M.P.
Canadian Journal of Chemistry, 1976 , vol. 54, p. 24 - 30
反应条件
1: With tert.-butyl lithium in diethyl ether; pentane
T=-20°C; 3 h;
2: With 1,2-di-iodoethane in diethyl ether; pentane
T=-78 - 20°C; 16 h;
参考文献
Gonzalez-Lopez De Turiso, Felix; Curran, Dennis P.
Organic Letters, 2005 , vol. 7, # 1 p. 151 - 154