[2-(甲硫基)乙基]苯合成路线 (共 22 条)
反应条件
methyl bromide; nitromethane
参考文献
Saunders; Asperger
Journal of the American Chemical Society, 1957 , vol. 79, p. 1612,1614
参考文献
Franzen,V.; Schmidt,H.-J.
Chemische Berichte, 1961 , vol. 94, p. 2937 - 2942
参考文献
v.Braun; Teuffert; Weissbach
Justus Liebigs Annalen der Chemie, 1929 , vol. 472, p. 131
反应条件
n-butyllithium; carbon dioxide 1.) Et2O, hexane, reflux, 4 h, 2.) Et2O, hexane, 15 h; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Cabiddu, S.; Floris, C.; Melis, S.; Piras, P. P.; Sotgiu, F.
Journal of Organometallic Chemistry, 1982 , vol. 236, # 2 p. 149 - 156
反应条件
carbon dioxide 1.) Et2O, hexane, reflux, 4 h, 2.) Et2O, hexane, 15 h; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Cabiddu, S.; Floris, C.; Melis, S.; Piras, P. P.; Sotgiu, F.
Journal of Organometallic Chemistry, 1982 , vol. 236, # 2 p. 149 - 156
反应条件
in tetrahydrofuran
T=0 - 20°C; Inert atmosphereGreen chemistry;
参考文献
Reeves, Jonathan T.; Camara, Kaddy; Han, Zhengxu S.; Xu, Yibo; Lee, Heewon; Busacca, Carl A.; Senanayake, Chris H.
Organic Letters, 2014 , vol. 16, # 4 p. 1196 - 1199
反应条件
sodium in methanol
Inert atmosphere;
参考文献
Rioz-Martinez, Ana; Kopacz, Malgorzata; De Gonzalo, Gonzalo; Torres Pazmino, Daniel E.; Gotor, Vicente; Fraaije, Marco W.
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 5 p. 1337 - 1341
反应条件
in methanol
Heating / reflux;
参考文献
THE BOARD OF TRUSTEES OF THE UNIVERSITY OF ILLINOIS
Patent: WO2007/109585 A2, 2007 ;
Location in patent: Page/Page column 47 ;
WO 2007/109585 A2
反应条件
1,4-diaza-bicyclo[2.2.2]octane in dichloromethane
T=0°C; 3 h;
参考文献
Barton, Derek H. R.; Jaszberenyi, Joseph Cs.; Theodorakis, Emmanouil A.
Tetrahedron, 1991 , vol. 47, # 44 p. 9167 - 9178
反应条件
methanol; sodium methylate
参考文献
Bacon; LeSuer
Journal of the American Chemical Society, 1954 , vol. 76, p. 670,671,674