hydrogen; tris(4-(1H,1H,2H,2H-perfluorodecyl)phenyl)phosphite; Ph(acac)(CO)2 in toluene T=80°C; P=30002.4 Torr; 2.5 h; Title compound not separated from byproducts;
Marinescu, Smaranda C.; Levine, Daniel S.; Zhao, Yu; Schrock, Richard R.; Hoveyda, Amir H.
Journal of the American Chemical Society, 2011 , vol. 133, # 30 p. 11512 - 11514
1: (C6H3(CH(CH3)2)2N)Mo(NC4H2(CH3)2)(CHC(CH3)2C6H5)(OC20H18Br2OSi(CH3)2C(CH3)3); ethene / benzene-d6 / 0.25 h / 22 °C / 3040.2 Torr / Inert atmosphere 2: (C6H3(CH(CH3)2)2N)Mo(NC4H2(CH3)2)(CHC(CH3)2C6H5)(OC20H18Br2OSi(CH3)2C(CH3)3); ethene / 0.92 h / 22 °C / 15201 Torr / Inert atmosphere View Scheme
参考文献
Marinescu, Smaranda C.; Levine, Daniel S.; Zhao, Yu; Schrock, Richard R.; Hoveyda, Amir H.
Journal of the American Chemical Society, 2011 , vol. 133, # 30 p. 11512 - 11514
