1: -263.16 °C / Irradiation; Inert atmosphere 2: -263.16 °C / Irradiation; Inert atmosphere View Scheme
参考文献
Pharr, Caroline R.; Kopff, Laura A.; Bennett, Brian; Reid, Scott A.; McMahon, Robert J.
Journal of the American Chemical Society, 2012 , vol. 134, # 14 p. 6443 - 6454
1: With sodium hydride in tetrahydrofuran; mineral oil
T=20°C; 1 h;
2: T=110°C;
参考文献
Pharr, Caroline R.; Kopff, Laura A.; Bennett, Brian; Reid, Scott A.; McMahon, Robert J.
Journal of the American Chemical Society, 2012 , vol. 134, # 14 p. 6443 - 6454
1.1: methanol / 12 h / Reflux
2.1: sodium hydride / tetrahydrofuran; mineral oil / 1 h / 20 °C
2.2: 110 °C
View Scheme
参考文献
Pharr, Caroline R.; Kopff, Laura A.; Bennett, Brian; Reid, Scott A.; McMahon, Robert J.
Journal of the American Chemical Society, 2012 , vol. 134, # 14 p. 6443 - 6454
