N-(4-溴苯基)-3-(4-氯苯基)磺酰基-2,,5-二甲基苯磺酰胺合成路线 (共 4 条)
反应条件
in water T=25°C; Equilibrium constant;
参考文献
Godoy-Alcantar; Yatsimirsky, Anatoly K.; Lehn
Journal of Physical Organic Chemistry, 2005 , vol. 18, # 10 p. 979 - 985
反应条件
Amberlite IRA-400(OH-) in ethanol 5 h; Heating;
参考文献
Konwar, Dilip; Dutta, Dilip Kumar; Goswami, Birendra Nath
Journal of Chemical Research - Part S, 1998 , # 6 p. 342 - 343
反应条件
1: 92 percent / diethyl ether; hexane / 1 h / -30 - 0 °C
2: 96 percent / DDQ
3: 92 percent / aq. HCl / methanol
View Scheme
参考文献
Strekowski, Lucjan; Wydra, Roman L.; Cegla, Marek T.; Czarny, Agnieszka; Patterson, Steven
Journal of Organic Chemistry, 1989 , vol. 54, # 26 p. 6120 - 6123
反应条件
1: With KPF6; [Ru(II)(η6-benzene)(μ-Cl)Cl]2; sodium hydroxide in acetonitrile
T=45°C; 48 h; Inert atmosphere;
2: With water; iodine in acetonitrile
T=20°C; 48 h; Inert atmosphere;
参考文献
Cuesta, Luciano; Maluenda, Irene; Soler, Tatiana; Navarro, Rafael; Urriolabeitia, Esteban P.
Inorganic Chemistry, 2011 , vol. 50, # 1 p. 37 - 45