2-(2-丙炔氧基)苯羧酸甲酯合成路线 (共 7 条)
反应条件
potassium carbonate in acetonitrile 24 h; Heating;
参考文献
Heterocycles, , vol. 48, # 12 p. 2611 - 2619
反应条件
1: 2-O-(prop-2-ynyl) salicylic acid With sodium in methanol Salt formation; 0.0833333 h; 2: propargyl bromide; 2-hydroxybenzoic acid methyl ester With potassium carbonate in acetone Alkylation; 16 h; Heating; Further stages.;
参考文献
Journal of the Chemical Society, Perkin Transactions 1, , # 5 p. 775 - 779
反应条件
[Ni(2,2'-bipyridine)3(2+)][BF4(1-)]2 in N,N-dimethyl-formamide Ambient temperatureelectrolysis;
参考文献
Olivero, Sandra; Dunach, Elisabet
Tetrahedron Letters, 1997 , vol. 38, # 35 p. 6193 - 6196
反应条件
potassium hydroxide; water in methanol T=20°C; Hydrolysis; 24 h;
参考文献
Chaudhuri, Gopeswar; Kundu, Nitya G.
Journal of the Chemical Society, Perkin Transactions 1, 2000 , # 5 p. 775 - 779
反应条件
1: 73 percent / H2O, KOH / ethanol / 25 h / Ambient temperature
2: SOCl2 / 0.5 h / Heating
View Scheme
参考文献
Pinho Melo, Teresa M. V.; Barbosa, Dalia M.; Ramos, Paulo J. R. S.; Rocha Gonsalves, Antonio M.; Gilchrist, Thomas L.; Beja, Ana M.; Paixaeo, Jose A.; Silva, Manuela R.; Veiga, Luiz Alte Da
Journal of the Chemical Society - Perkin Transactions 1, 1999 , # 9 p. 1219 - 1223
反应条件
[MeCNAu((1,1′-biphenyl-2-yl)-di-tert-butylphosphine)]+SbF6− in dichloromethane
T=18°C; 2 h; Inert atmosphere;
参考文献
Menon, Rajeev S.; Findlay, Alison D.; Bissember, Alex C.; Banwell, Martin G.
Journal of Organic Chemistry, 2009 , vol. 74, # 22 p. 8901 - 8903
反应条件
[MeCNAu((1,1′-biphenyl-2-yl)-di-tert-butylphosphine)]+SbF6−
参考文献
Lykakis, Ioannis N.; Efe, Christina; Gryparis, Charis; Stratakis, Manolis
European Journal of Organic Chemistry, 2011 , # 12 p. 2334 - 2338