4,4-二甲基-2-戊酮合成路线 (共 111 条)
反应条件
Catalyst M-Chromium oxide; sulfuric acid
参考文献
Journal of the American Chemical Society, , vol. 74, p. 3228
Zhurnal Obshchei Khimii, , vol. 3, p. 253
Bulletin de la Societe Chimique de France, , vol. <4>53, p. 328
US2004066 , ;
Journal of the American Chemical Society, , vol. 55, p. 4209,4212
反应条件
Nitrous oxide T=290°C; P=37503.8 Torr; 24 h; AutoclaveInert atmosphere;
参考文献
US2011/269996 A1, ;
Page/Page column 5 ;
参考文献
Journal of the American Chemical Society, , vol. 68, p. 1653
参考文献
Journal of the American Chemical Society, , vol. 68, p. 1653
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide; chloro-trimethyl-silane; lithium iodide in various solvent(s) -78 deg C, 1 h, 0 deg C, 0.1 h;
参考文献
Bertz, Steven H.; Dabbagh, Gary
Tetrahedron, 1989 , vol. 45, # 2 p. 425 - 434
反应条件
tetrabutyl ammonium fluoride in tetrahydrofuran 1 h; Ambient temperature;
参考文献
Dang, Hai-Shan; Roberts, Brian P.
Journal of the Chemical Society - Perkin Transactions 1, 1996 , # 8 p. 769 - 775
反应条件
Nitrous oxide T=290°C; P=37503.8 Torr; 24 h; AutoclaveInert atmosphere; Product distribution / selectivity;
参考文献
US2011/269996 A1, ;
Page/Page column 5 ;
反应条件
ozone in pentane T=-60°C; 1.33333 h; Title compound not separated from byproducts;
参考文献
Organic and Biomolecular Chemistry, , vol. 3, # 7 p. 1323 - 1329
反应条件
in benzene 1 h; Irradiation; Further byproducts given. Yields of byproduct given;
参考文献
Alender, Jeffrey; Morgan, Peter; Timberlake, Jack
Journal of Organic Chemistry, 1983 , vol. 48, # 5 p. 755 - 756
反应条件
Nitrous oxide T=300°C; P=367754 Torr;
参考文献
Journal of the Chemical Society, , p. 2999,3006