2-甲基-3-戊炔-2-醇合成路线 （共 29 条）
反应条件
copper(l) iodide; triethylamine; triphenylphosphine; bis-triphenylphosphine-palladium(II) chloride
Sonogashira coupling reaction; 24 h; Heating;
参考文献
Xing, Jin-Feng; Chen, Wei-Qiang; Gu, Jie; Dong, Xian-Zi; Takeyasu, Nobuyuki; Tanaka, Takuo; Duan, Xuan-Ming; Kawata, Satoshi
Journal of Materials Chemistry, 2007 , vol. 17, # 14 p. 1433 - 1438
反应条件
N-ethyl-N,N-diisopropylamine; trifluoroacetic anhydride in dichloromethane
1) -78 deg C, 2) -40 deg C, 30 min;
参考文献
Hoffmann, H. M. R.; Matthei, Juergen
Chemische Berichte, 1980 , vol. 113, # 12 p. 3837 - 3847
反应条件
N-ethyl-N,N-diisopropylamine in dichloromethane
1) -78 deg C, 2) -40 deg C, 30 min;
参考文献
Hoffmann, H. M. R.; Matthei, Juergen
Chemische Berichte, 1980 , vol. 113, # 12 p. 3837 - 3847
参考文献
Bobrovnikov, M. N.; Turbanova, E. S.; Petrov, A. A.
Russian Journal of Organic Chemistry, 1993 , vol. 29, # 9.1 p. 1445 - 1449
Zhurnal Organicheskoi Khimii, 1993 , vol. 29, # 9 p. 1739 - 1745
反应条件
hydrogenchloride; calcium chloride in Petroleum ether
参考文献
Mayr, Herbert; Halberstadt-Kausch, Inge K.
Chemische Berichte, 1982 , vol. 115, # 11 p. 3479 - 3515
参考文献
Hurd; Cohen
Journal of the American Chemical Society, 1931 , vol. 53, p. 1073
参考文献
Sacharowa
Zhurnal Obshchei Khimii, 1947 , vol. 17, p. 689
Chem.Abstr., 1948 , p. 1871
反应条件
1: HCl
2: glacial acetic acid / 60 °C
View Scheme
参考文献
Sacharowa
Zhurnal Obshchei Khimii, 1947 , vol. 17, p. 689
Chem.Abstr., 1948 , p. 1871
参考文献
Sacharowa
Zhurnal Obshchei Khimii, 1947 , vol. 17, p. 689
Chem.Abstr., 1948 , p. 1871
