2-甲基-3-戊炔-2-醇合成路线 (共 29 条)
反应条件
1: aq. HCl / 0 °C View Scheme
参考文献
Bianchini,J.-P.; Guillemonat,J.-C.
Comptes Rendus des Seances de l'Academie des Sciences, Serie C: Sciences Chimiques, 1968 , vol. 266, p. 214 - 216
参考文献
Mkryan,G.M. et al.
Zhurnal Organicheskoi Khimii, 1970 , vol. 6, p. 912 - 915,917 - 920
反应条件
ReOCl3(SMe2)(OPPh3); ethyl acetate T=70°C; Meyer-Schuster Rearrangement; 20 h;
参考文献
Garst, Alyson E.; Badiceanu, Alexandra D.; Nolin, Kristine A.
Tetrahedron Letters, 2013 , vol. 54, # 6 p. 459 - 461
反应条件
1: NaOH 2: dibutyl ether View Scheme
参考文献
Bianchini,J.-P.; Guillemonat,J.-C.
Comptes Rendus des Seances de l'Academie des Sciences, Serie C: Sciences Chimiques, 1968 , vol. 266, p. 214 - 216
反应条件
1: calcium chloride; hydroquinone; petroleum ether; hydrogen chloride / 0 °C 2: lithium alanate; dioxane View Scheme
参考文献
Fantazier,R.M.; Poutsma,M.L.
Journal of the American Chemical Society, 1968 , vol. 90, p. 5490 - 5498
参考文献
Tamaru; Kimura; Tanaka; Kure; Yoshida
Bulletin of the Chemical Society of Japan, 1994 , vol. 67, # 10 p. 2838 - 2849
反应条件
ammonia; lithium; iron nitrate (III) in diethyl ether
T=-40°C; 1 h;
参考文献
Mayr, Herbert; Halberstadt-Kausch, Inge K.
Chemische Berichte, 1982 , vol. 115, # 11 p. 3479 - 3515
反应条件
diethyl ether
T=0°C;
参考文献
Sacharowa
Zhurnal Obshchei Khimii, 1947 , vol. 17, p. 689
Chem.Abstr., 1948 , p. 1871
Full Text Show Details
Hurd; Cohen
Journal of the American Chemical Society, 1931 , vol. 53, p. 1073
反应条件
potassium hydroxide; diethyl ether
T=0°C;
参考文献
Sacharowa
Zhurnal Obshchei Khimii, 1947 , vol. 17, p. 689
Chem.Abstr., 1948 , p. 1871
反应条件
sulfuric acid in diethyl ether
参考文献
Andrews,S.D. et al.
Journal of the Chemical Society [Section] C: Organic, 1969 , p. 2443 - 2449