反应条件
1: 1) AlCl3, NaCl, 2) conc. HCl, H2O / 1) melt, 180 deg C, 2) 0 deg C, 3 h 2: 90 percent / Zn / pyridine 3: 91 percent / NaOAc, H2 / Pd/C (10 percent Pd) / methanol / 10 h / 40 - 45 °C / Irradiation 4: 73 percent / 1) 2 N NaOH, 2) FeCl3*6H2O/HCl / 1) MeOH, reflux, 2) H2O 5: 98 percent / Ag2O / CHCl3 / Heating 6: Na2S2O4 / diethyl ether; CHCl3; H2O 7: 83 percent / 1) HCl, 2) H2O / 1) 15 min 8: 1) Ag2O, (Et)3N (0.3 percent), 2) HNO3 (65 percent) / 1) CHCl3, 2) 2 min View Scheme
参考文献
Laatsch, Hartmut
Liebigs Annalen der Chemie, 1980 , # 8 p. 1321 - 1347
