(2,4-二甲基苯基)-磷酸二乙酯合成路线 （共 7 条）
参考文献
Rudinskas,A.J.; Hullar,T.L.
Journal of Organic Chemistry, 1976 , vol. 41, p. 2411 - 2417
反应条件
palladium diacetate in acetonitrile
T=160°C; 0.75 h; Microwave irradiationsealed vessel;
参考文献
IDENIX PHARMACEUTICALS, INC.; DOUSSON, Cyril; SURLERAUX, Dominique; PAPARIN, Jean-laurent; PIERRA, Claire; GRIFFON, Jean-francois; LEROY, Frederic; DUKHAN, David
Patent: WO2010/101967 A2, 2010 ;
Location in patent: Page/Page column 145 ;
反应条件
α-cyclohexylcyclohexanemethanamine; triphenylphosphine; palladium diacetate in ethanol
T=76°C; 16 h;
参考文献
Goossen, Lukas J.; Dezfuli, Mohammad K.
Synlett, 2005 , # 3 art. no. G45204ST, p. 445 - 448
反应条件
CAN in acetic acid
5 h; Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Kottmann, Hariolf; Skarzewski, Jacek; Effenberger, Franz
Synthesis, 1987 , # 9 p. 797 - 801
反应条件
Mn(OAc)3•2H2O in acetic acid
T=60°C; 7 h;
参考文献
Xu, Wei; Zou, Jian-Ping; Zhang, Wei
Tetrahedron Letters, 2010 , vol. 51, # 19 p. 2639 - 2643
反应条件
CAN in acetonitrile
5 h; Ambient temperature; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Kottmann, Hariolf; Skarzewski, Jacek; Effenberger, Franz
Synthesis, 1987 , # 9 p. 797 - 801
反应条件
1.) anodic oxidation acetonitrile, graphite electrodes, Bu4NClO4, 1180 mV 2.) work up with nucleophile; Yield given. Multistep reaction. Title compound not separated from byproducts;
参考文献
Effenberger, Franz; Kottmann, Hariolf
Tetrahedron, 1985 , vol. 41, # 19 p. 4171 - 4182
