N,N-二乙基-4-溴苯甲酰胺合成路线 （共 13 条）
反应条件
triethylamine in dichloromethane T=-10 - 20°C; 0.5 h;
参考文献
General Electric Company
Patent: US2008/27028 A1, 2008 ;
Location in patent: Page/Page column 35-36 ;
反应条件
tert.-butylhydroperoxide; tetra-(n-butyl)ammonium iodide in trichloroethane, 1,1,2-; water T=90°C; 12 h;
参考文献
Li, Huamin; Xie, Jin; Xue, Qicai; Cheng, Yixiang; Zhu, Chengjian
Tetrahedron Letters, 2012 , vol. 53, # 48 p. 6479 - 6482,4
反应条件
dipotassium peroxodisulfate; palladium diacetate in water; dimethyl sulfoxide; acetonitrile T=20°C;
参考文献
Li, Mingzong; Wang, Cong; Fang, Ping; Ge, Haibo
Chemical Communications, 2011 , vol. 47, # 23 p. 6587 - 6589
反应条件
copper(I) oxide; 1,10-phenanthroline; oxygen; toluene-4-sulfonic acid T=140°C; P=760.051 Torr; 24 h; Sealed tube;
参考文献
Organic and Biomolecular Chemistry, , vol. 11, # 47 p. 8179 - 8182
反应条件
1: thionyl chloride; N,N-dimethyl-formamide / toluene / 20 °C 2: triethylamine / dichloromethane / 0 - 20 °C View Scheme
参考文献
Organic Letters, , vol. 16, # 2 p. 390 - 393
反应条件
in acetonitrile 2 h; Ambient temperature; Yield given;
参考文献
Journal of Organic Chemistry, , vol. 46, p. 4413 - 4416
反应条件
tris(dibenzylideneacetone)dipalladium (0); lithium hexamethyldisilazane; 2-dicyclohexylphosphino-1,1'-biphenyl in 1,4-dioxane T=80°C; 15 h;
参考文献
Huang; Buchwald
Organic letters, 2001 , vol. 3, # 21 p. 3417 - 3419
反应条件
zirconocene dichloride; lithium tri-t-butoxyaluminum hydride in tetrahydrofuran T=20°C; 0.0333333 h; Product distribution / selectivity;
参考文献
Zhao, Yigang; Snieckus, Victor
Organic Letters, 2014 , vol. 16, # 2 p. 390 - 393
反应条件
C80H88Cl2N6NiP2 in tetrahydrofuran T=25°C; Kumada coupling reaction; 4 h; Inert atmosphere;
参考文献
Xie, Lan-Gui; Wang, Zhong-Xia
Chemistry - A European Journal, 2010 , vol. 16, # 34 p. 10332 - 10336
