5-甲氧基-2-苯基-1H-吲哚合成路线 （共 43 条）
反应条件
1: 62 percent / sodium ethoxide / dimethylsulfoxide / 24 h / Ambient temperature 2: 78 percent / iron powder, conc. hydrochloric acid / methanol; H2O / 24 h / Heating 3: 77 percent / allyl methyl carbonate, dihydridotetrikis(triphenylphosphine)ruthenium(II) / toluene / 24 h / 100 °C View Scheme
参考文献
Journal of Heterocyclic Chemistry, , vol. 29, # 5 p. 1085 - 1090
反应条件
1: 62 percent / sodium ethoxide / dimethylsulfoxide / 24 h / Ambient temperature 2: 78 percent / iron powder, conc. hydrochloric acid / methanol; H2O / 24 h / Heating 3: 77 percent / allyl methyl carbonate, dihydridotetrikis(triphenylphosphine)ruthenium(II) / toluene / 24 h / 100 °C View Scheme
参考文献
Journal of Heterocyclic Chemistry, , vol. 29, # 5 p. 1085 - 1090
反应条件
1: 78 percent / iron powder, conc. hydrochloric acid / methanol; H2O / 24 h / Heating 2: 77 percent / allyl methyl carbonate, dihydridotetrikis(triphenylphosphine)ruthenium(II) / toluene / 24 h / 100 °C View Scheme
参考文献
Journal of Heterocyclic Chemistry, , vol. 29, # 5 p. 1085 - 1090
反应条件
tetrakis(triphenylphosphine) palladium(0); sodium carbonate in 1,4-dioxane Suzuki coupling; Reflux;
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 20, # 8 p. 2586 - 2590
反应条件
1: 41.6 percent / sodium hydroxide / ethanol / 0.5 h / 80 °C 2: diethyl ether / 2 h / 20 °C View Scheme
参考文献
Synthetic Communications, , vol. 35, # 20 p. 2625 - 2632
反应条件
1: acetic acid / ethanol / 100 °C 2: 1-propanephosphonic acid cyclic anhydride / toluene / 120 °C View Scheme
参考文献
Chemical Communications, , vol. 49, # 74 p. 8196 - 8198
反应条件
in N,N-dimethyl acetamide T=170°C;
参考文献
Bioorganic and Medicinal Chemistry, , vol. 22, # 2 p. 787 - 795
反应条件
1: 1) lithium 2,2,6,6-tetramethylpiperidide / 1) -10 deg C, THF, 2) 0 deg C, 20 min 2: 1) lithium 2,2,6,6-tetramethylpiperidide / 1) -10 degC, THF, 2) 0 degC, 20 min View Scheme
参考文献
Tetrahedron, , vol. 46, # 4 p. 1379 - 1384
反应条件
1: 1) lithium 2,2,6,6-tetramethylpiperidide / 1) -10 degC, THF, 2) 0 degC, 20 min 2: 1) lithium 2,2,6,6-tetramethylpiperidide / 1) -10 degC, THF, 2) 0 degC, 20 min View Scheme
参考文献
Tetrahedron, , vol. 46, # 4 p. 1379 - 1384
反应条件
1: 1) lithium 2,2,6,6-tetramethylpiperidide / 1) -10 degC, THF, 2) 0 degC, 20 min 2: 1) lithium 2,2,6,6-tetramethylpiperidide / 1) -10 degC, THF, 2) 0 degC, 20 min View Scheme
参考文献
Tetrahedron, , vol. 46, # 4 p. 1379 - 1384
