2,4-二苯基-3-丁炔-2-醇合成路线 （共 18 条）
反应条件
potassium tert-butylate in neat (no solvent)
T=20°C; 0.5 h; Reagent/catalystTime;
参考文献
Chen, Shufeng; Yuan, Fang; Zhao, Haiying; Li, Baoguo
Research on Chemical Intermediates, 2013 , vol. 39, # 6 p. 2391 - 2399
反应条件
in toluene
T=80°C; 5 h;
参考文献
Baidossi, Wael; Rosenfeld, Ayelet; Wassermann, Brigit C.; Schutte, Stefan; Schumann, Herbert; Blum, Jochanan
Synthesis, 1996 , # 9 p. 1127 - 1130
反应条件
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; triphenylphosphine
Inert atmosphereSealed flaskHeating;
参考文献
Zhou, Chao; Chen, Xiaopeng; Lu, Ping; Wang, Yanguang
Tetrahedron, 2012 , vol. 68, # 13 p. 2844 - 2850
反应条件
hydrogenchloride in ethanol
0.0666667 h;
参考文献
Komissarova; Aleksandrova; Stadnichuk
Russian Journal of General Chemistry, 1997 , vol. 67, # 3 p. 412 - 416
反应条件
in tetrahydrofuran
T=20 - 23°C;
参考文献
Potkin; Dikusar; Kozlov
Russian Journal of Organic Chemistry, 2002 , vol. 38, # 9 p. 1260 - 1265
反应条件
indium in dichloromethane
0.4 h; Heating;
参考文献
Auge, Jacques; Lubin-Germain, Nadege; Seghrouchni, Latifa
Tetrahedron Letters, 2002 , vol. 43, # 30 p. 5255 - 5256
参考文献
Adegoke, Emmanuel A.; Emokpae, T. A.; Ephraim-Bassey, H.; Oyelola, C. A.
Journal of Heterocyclic Chemistry, 1987 , vol. 24, p. 1705 - 1708
反应条件
1: With dimethyl sulfoxide; potassium hydroxide
T=20°C; 1 h;
2: With water in dimethyl sulfoxide
参考文献
Trofimov, Boris A.; Schmidt, Elena Yu; Ushakov, IgoR'A; Zorina, Nadezhda V.; Skital'Tseva, Elena V.; Protsuk, Nadezhda I.; Mikhaleva, AL'Bina I.
Chemistry - A European Journal, 2010 , vol. 16, # 28 p. 8516 - 8521
反应条件
1: diethyl ether; sodium
2: absolute diethyl ether / Zersetzung mit Schwefelsaeure
View Scheme
参考文献
Nef
Justus Liebigs Annalen der Chemie, 1899 , vol. 308, p. 325
反应条件
1: natrium carbonate
2: diethyl ether; sodium
3: absolute diethyl ether / Zersetzung mit Schwefelsaeure
View Scheme
参考文献
Nef
Justus Liebigs Annalen der Chemie, 1899 , vol. 308, p. 325
