4-溴-4′-甲氧基联苯合成路线 （共 57 条）
反应条件
ethyl bromide; magnesium in diethyl ether
参考文献
Surendranath, V.; Fishel, D. L.; Vries, A de; Mahmood, R.; Johnson, D. L.
Molecular Crystals and Liquid Crystals (1969-1991), 1985 , vol. 131, p. 1 - 8
反应条件
1: 40 percent / copper powder / dimethylformamide / 20 h / 150 °C / in autoclave 2: 79 percent / (CH3)3SiI / CHCl3 / 120 h / 20 °C View Scheme
参考文献
Barny, P. le; Ravaux, G.; Dubois, J. C.; Parneix, J. P.
Molecular Crystals and Liquid Crystals (1969-1991), 1985 , vol. 127, p. 413 - 430
参考文献
Spivey, Alan C.; Diaper, Christopher M.; Rudge, Andrew J.
Chemical Communications, 1999 , # 9 p. 835 - 836
反应条件
n-butyllithium; boric acid trimethyl ester; N,N,N',N,-tetramethylethylenediamine in tetrahydrofuran T=20°C; 1 h;
参考文献
Journal of Heterocyclic Chemistry, , vol. 44, # 4 p. 853 - 862
反应条件
copper in N,N-dimethyl-formamide
T=150°C; 20 h; in autoclave;
参考文献
Barny, P. le; Ravaux, G.; Dubois, J. C.; Parneix, J. P.
Molecular Crystals and Liquid Crystals (1969-1991), 1985 , vol. 127, p. 413 - 430
反应条件
1: Mg, C2H5Br / diethyl ether
2: 48percent HBr / acetic acid
3: H(+) / toluene
View Scheme
参考文献
Surendranath, V.; Fishel, D. L.; Vries, A de; Mahmood, R.; Johnson, D. L.
Molecular Crystals and Liquid Crystals (1969-1991), 1985 , vol. 131, p. 1 - 8
参考文献
Spivey, Alan C.; Diaper, Christopher M.; Rudge, Andrew J.
Chemical Communications, 1999 , # 9 p. 835 - 836
