4-甲氧基-4’-氰基联苯合成路线 (共 80 条)
反应条件
in water; acetone; tert-butyl alcohol Irradiation;
参考文献
Tetrahedron, , vol. 33, p. 779 - 786
反应条件
in water; acetone; tert-butyl alcohol Irradiation;
参考文献
Tetrahedron, , vol. 33, p. 779 - 786
反应条件
in methanol 1 h; Irradiation; Yield given. Title compound not separated from byproducts;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 1 p. 141 - 146
反应条件
1: With diisobutylaluminium hydride in dichloromethane T=0 - 20°C; 19 h; 2: With hydrogenchloride; water in dichloromethane T=20°C;
参考文献
WO2005/30702 A1, ;
Page/Page column 47 ;
反应条件
1: hydrolysis 2: demethylation View Scheme
参考文献
Goodby, J. W.; Patel, J. S.; Chin, E.
Journal of Physical Chemistry, 1987 , vol. 91, # 20 p. 5151 - 5152
反应条件
1: 80 percent / AlI3 / acetonitrile / 5 h / Heating 2: 85 percent / K2CO3 / acetone / 6 h / Heating View Scheme
参考文献
Heinrich, B.; Guillon, D.
Molecular Crystals and Liquid Crystals Science and Technology, Section A: Molecular Crystals and Liquid Crystals, 1995 , vol. 268, p. 21 - 44
反应条件
sulfuric acid; water in acetic acid 6 h; Heating / reflux;
参考文献
The Secretary of State for Defence in Her Britannic Majesty's Government of the United Kingdom of Great Britain and Northern Ireland Defence Evaluation Research Agency
Patent: US6337420 B1, 2002 ;
Location in patent: Page column 6 ;
反应条件
1: 80 percent / AlI3 / acetonitrile / 5 h / Heating 2: 85 percent / K2CO3 / acetone / 6 h / Heating 3: 25percent aq. KOH / propan-2-ol / 1 h / Heating 4: 25percent aq. KOH / propan-2-ol / 96 h / Heating View Scheme
参考文献
Heinrich, B.; Guillon, D.
Molecular Crystals and Liquid Crystals Science and Technology, Section A: Molecular Crystals and Liquid Crystals, 1995 , vol. 268, p. 21 - 44
反应条件
boron tribromide in dichloromethane T=20°C; Cooling with ice;
参考文献
Moorthy, Jarugu Narasimha; Koner, Apurba L.; Samanta, Subhas; Roy, Ankur; Nau, Werner M.
Chemistry - A European Journal, 2009 , vol. 15, # 17 p. 4289 - 4300
反应条件
pyridine; hydrogenchloride
参考文献
Societe d'Expansion Scientifique Expansia
Patent: US6046352 A1, 2000 ;