4-苄基-2-苯基-2-噁唑啉-5-酮合成路线 （共 38 条）
反应条件
acetic acid in dichloromethane T=0°C; RefluxInert atmosphere;
参考文献
Metrano, Anthony J.; Miller, Scott J.
Journal of Organic Chemistry, 2014 , vol. 79, # 4 p. 1542 - 1554
反应条件
1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride in dichloromethane T=0 - 20°C;
参考文献
Organic Letters, , vol. 13, # 19 p. 5060 - 5063
反应条件
1: in toluene T=0°C; 2 h; Inert atmosphere; 2: With triethylamine in toluene T=80°C; 10 h; Inert atmosphere;
参考文献
Weber, Manuel; Jautze, Sascha; Frey, Wolfgang; Peters, Rene
Chemistry - A European Journal, 2012 , vol. 18, # 46 p. 14792 - 14804
反应条件
1: NaOH / diethyl ether; H2O / pH=10-12 2: Ac2O View Scheme
参考文献
Tetrahedron Letters, , vol. 27, # 14 p. 1579 - 1582
反应条件
1: NaOH / diethyl ether; H2O / pH=10-12 2: Ac2O View Scheme
参考文献
Tetrahedron Letters, , vol. 27, # 14 p. 1579 - 1582
反应条件
hydrogen; triethylamine; palladium dichloride in tert-butyl alcohol Rate constant;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 32, # 8 p. 1575 - 1581
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 8 p. 1740 - 1747
反应条件
1: sodium hydroxide / water; acetone / 20 °C 2: N,N-diethylaniline hydrochloride; 4-(4,6-Dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholin-4-ium chloride / dichloromethane; water; acetone / 6 h / 20 °C View Scheme
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 60, # 7 p. 907 - 912
反应条件
1: 4-methyl-morpholine / water; acetone / 0.25 h / 20 °C 2: sodium hydroxide / water; acetone / 20 °C 3: N,N-diethylaniline hydrochloride; 4-(4,6-Dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholin-4-ium chloride / dichloromethane; water; acetone / 6 h / 20 °C View Scheme
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 60, # 7 p. 907 - 912
反应条件
oxalic acid in water; ethyl acetate
反应条件
1: 20 h / 60 °C 2: oxalic acid / 0.25 h / 110 - 120 °C View Scheme
参考文献
Liebigs Annalen der Chemie, , # 1 p. 1 - 6
