反应条件
1: Na(CN)BH3, AcOH / Ambient temperature
2: aq. 70percent HNO3, H2SO4 / 0.08 h / 0 °C
3: H2 / 10percent Pd/C / ethyl acetate; ethanol / 5 h / 760 Torr
4: ZnCl2 / ethanol / 16 h / Heating
5: Na(CN)BH3, AcOH / Ambient temperature
View Scheme
参考文献
Edwards, James P.; West, Sarah J.; Pooley, Charlotte L. F.; Marschke, Keith B.; Farmer, Luc J.; Jones, Todd K.
Bioorganic and Medicinal Chemistry Letters, 1998 , vol. 8, # 7 p. 745 - 750