反应条件
1: 1) LiNH2 / 1) liq. NH3, THF, 2 h; 2) THF, 3 h
2: 60 percent / LiAlH4 / diethyl ether / 1) 1 h; 2) 5 h, reflux
3: 70 percent / PBr3, pyridine / diethyl ether / 1) overnight, 2) reflux, 2 h
4: 1) Mg / 2)Li2CuCl4 / 1) THF, 2) THF, -10 deg C, 5 h
5: 50 percent / pTsOH / methanol / 6 h / 55 °C
6: 60 percent / PCC / CH2Cl2 / 2 h
View Scheme
参考文献
Sharma; Sabharwal; Vohra; Vig; Kad
Journal of the Indian Chemical Society, 1990 , vol. 67, # 1 p. 31 - 33
