1,3-双(4-硝基苯基)脲合成路线 （共 71 条）
反应条件
in 1,4-dioxane T=100°C; 24 h;
参考文献
Boiocchi, Massimo; Del Boca, Laura; Gomez, David Esteban; Fabbrizzi, Luigi; Licchelli, Maurizio; Monzani, Enrico
Journal of the American Chemical Society, 2004 , vol. 126, # 50 p. 16507 - 16514
反应条件
caesium carbonate; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene; tris(dibenzylideneacetone)dipalladium(0) chloroform complex in 1,4-dioxane T=100°C; 4 h;
参考文献
Artamkina; Sergeev; Beletskaya
Russian Journal of Organic Chemistry, 2002 , vol. 38, # 4 p. 538 - 545
反应条件
4-(N,N-dimethlyamino)pyridine in toluene T=80 - 90°C; 6 h;
参考文献
CHEMAGIS LTD.; PERRIGO COMPANY
Patent: WO2007/70804 A2, 2007 ;
Location in patent: Page/Page column 20-21 ;
反应条件
4-(N,N-dimethlyamino)pyridine; W(CO)6; iodine in dichloromethane T=40°C; P=60804.1 Torr; 8 h;
参考文献
Zhang, Li; Darko, Ampofo K.; Johns, Jennifer I.; McElwee-White, Lisa
European Journal of Organic Chemistry, 2011 , # 31 p. 6261 - 6268
反应条件
water; triethylamine in 1,4-dioxane T=20°C; 0.05 h;
参考文献
Perveen, Shahnaz; Abdul Hai, Syed M.; Khan, Rashid A.; Khan, Khalid Mohammed; Afza, Nighat; Sarfaraz, Tahira B.
Synthetic Communications, 2005 , vol. 35, # 12 p. 1663 - 1674
反应条件
sulfuric acid; nitric acid T=0 - 100°C; 1 - 2 h; Heating / reflux; Product distribution / selectivity;
参考文献
Perveen, Shahnaz
Patent: US2008/221214 A1, 2008 ;
Location in patent: Page/Page column 1-2 ;
反应条件
zinc(II) chloride T=80 - 85°C; 0.133333 h; Neat (no solvent);
参考文献
Pasha; Madhusudana Reddy
Synthetic Communications, 2009 , vol. 39, # 16 p. 2928 - 2934
反应条件
potassium superoxide in dimethyl sulfoxide 3 h; Ambient temperature;
参考文献
KIM, Yong Hae; YON, Gyu Hwan; KIM, Hyung Jin
Chemistry Letters, 1984 , p. 309 - 312
反应条件
sodium carbonate; nitrobenzene
参考文献
Zhurnal Obshchei Khimii, , vol. 27, p. 2532,2533; engl.Ausg. S.2590,2591
参考文献
Journal fuer Praktische Chemie (Leipzig), , vol. <2> 52, p. 232
