乙基3-(2-甲基苯基)-2-丙炔酸酯合成路线 (共 4 条)
反应条件
T=120°C; P=1292.9 Torr; 0.15 h; Microwave irradiationSealed tube; Temperature;
参考文献
Komsani, Jayaram Reddy; Koppireddi, Satish; Avula, Sreenivas; Koochana, Pranay Kumar; Yadla, Rambabu
European Journal of Medicinal Chemistry, 2013 , vol. 68, p. 132 - 138
反应条件
copper(l) iodide; air; caesium carbonate; silver(l) oxide in dichloromethane
T=80°C; Sonogashira type reaction; 36 h;
参考文献
Pan, Changduo; Luo, Fang; Wang, Wenhui; Ye, Zhishi; Cheng, Jiang
Tetrahedron Letters, 2009 , vol. 50, # 35 p. 5044 - 5046
反应条件
T=500°C; P=0.1 - 1 Torr;
参考文献
Aitken, R. Alan; Horsburg, Caroline E. R.; McCreadie, J. Graeme; Seth, Shirley
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1994 , # 13 p. 1727 - 1732
反应条件
1: 64 percent / Et3N / toluene / 3 h / Ambient temperature
2: 90 percent / 500 °C / 0.1 - 1 Torr
View Scheme
参考文献
Aitken, R. Alan; Horsburg, Caroline E. R.; McCreadie, J. Graeme; Seth, Shirley
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1994 , # 13 p. 1727 - 1732