2-(4-异丁基苯基)丙腈合成路线 (共 25 条)
反应条件
1: 1) enzyme system from Rhodococcus butanica, 6 h 2) CH2N2 2: 6N H2SO4, AcOH / 12 h / Heating View Scheme
参考文献
Kakeya, Hideaki; Sakai, Naoko; Sugai, Takeshi; Ohta, Hiromichi
Tetrahedron Letters, 1991 , vol. 32, # 10 p. 1343 - 1346
反应条件
in water T=32°C; 120 h; nitrilase from Acinetobacter sp. AK 226, phosphate buffer pH 8.0, time course of the reaction, enantioselectrivity; Product distribution;
参考文献
Yamamoto; Komatsu
Agricultural and biological chemistry, 1991 , vol. 55, # 6 p. 1459 - 1466
反应条件
in water T=32°C; 120 h; nitrilase from Acinetobacter sp. AK 226, phosphate buffer pH 8.0, time course of the reaction, enantioselectrivity; Product distribution;
参考文献
Yamamoto; Komatsu
Agricultural and biological chemistry, 1991 , vol. 55, # 6 p. 1459 - 1466
反应条件
[Ru(η6-C6Me6)Cl2(tris(dimethylamino)phosphine)]; water T=150°C; 1 h; Inert atmosphereMicrowave irradiation;
参考文献
Garcia-Alvarez, Rocio; Diez, Josefina; Crochet, Pascale; Cadierno, Victorio
Organometallics, 2011 , vol. 30, # 20 p. 5442 - 5451
反应条件
potassium hydroxide in ethanol 16 h;
参考文献
Hiyama; Inoue; Saito
Synthesis, 1986 , vol. NO. 8, p. 645 - 647