反应条件
hydrogenchloride; n-butyllithium; bis(cyclopentadienyl)zirconium monomethylmonochloride 1.) THF, hexane, -50 deg C, 30 min, 2.) THF, -50 deg C, 15 min, 3.) THF, 80 deg C, 24 h, room temperature, 4 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Journal of the American Chemical Society, , vol. 109, p. 7137