4-羟基-2,6-二甲基苯腈合成路线 （共 5 条）
反应条件
tri-tert-butyl phosphine; zinc; tris(dibenzylideneacetone)dipalladium (0) in hexane; N,N-dimethyl-formamide T=20°C; 1 h;
参考文献
Ramnauth, Jailall; Bhardwaj, Namrta; Renton, Paul; Rakhit, Suman; Maddaford, Shawn P.
Synlett, 2003 , # 14 p. 2237 - 2239
反应条件
1: With potassium tert-butylate in tert-butyl alcohol T=120°C; 0.5 h; Microwave irradiation; 2: With hydrogenchloride in water; tert-butyl alcohol 1 h; Reflux;
参考文献
Marshall, Laura J.; Cable, Karl M.; Botting, Nigel P.
Journal of Labelled Compounds and Radiopharmaceuticals, 2010 , vol. 53, # 5-6 p. 457 - 459
参考文献
Fortsch. Ch. Phys., vol. 18, p. Heft 2, S. 23
反应条件
potassium cyanide; samarium diiodide; 18-crown-6 ether 1.) CH2Cl2, room t., 20 min, 2.) THF, MeOH, -78 deg C; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Tetrahedron Letters, , vol. 35, # 43 p. 7901 - 7904
参考文献
Houben; Fischer
Chemische Berichte, 1933 , vol. 66, p. 339,344
