3,4-二乙酰氧基苯甲酸合成路线 （共 25 条）
参考文献
Ciamician; Silber
Chemische Berichte, 1892 , vol. 25, p. 1472
反应条件
piperidine; diethyl ether; ethanol
参考文献
Journal of the American Chemical Society, , vol. 52, p. 4012
参考文献
Journal of the American Chemical Society, , vol. 52, p. 4012
反应条件
1: 82 percent / SOCl2, pyridine / 1.5 h / Heating 2: TEA / dioxane 3: 2 N etheric HCl / dioxane / 0.25 h / 20 °C View Scheme
参考文献
Schmidt, Ulrich; Wild, Jochen
Liebigs Annalen der Chemie, 1985 , # 9 p. 1882 - 1894
反应条件
1.1: thionyl chloride / N,N-dimethyl-formamide / 4 h / |Reflux 1.2: 20 °C 2.1: 1-methylguanidine hydrochloride; triethylamine / dichloromethane; methanol / 2 h View Scheme
参考文献
LeBlanc, Luc M.; Pare, Aurelie F.; Jean-Francois, Jacques; Hebert, Martin J.G.; Surette, Marc E.; Touaibia, Mohamed
Molecules, 2012 , vol. 17, # 12 p. 14637 - 14650
反应条件
pyridine
T=0°C; 2 h; Inert atmosphere;
参考文献
Zhang, Qingzhi; Raheem, K. Saki; Botting, Nigel P.; Slawin, Alexandra M.Z.; Kay, Colin D.; O'Hagan, David
Tetrahedron, 2012 , vol. 68, # 22 p. 4194 - 4201
反应条件
hydrogenchloride; potassium hydroxide; acetic anhydride in ethyl acetate
参考文献
Kureha Kagaku Kogyo Kabushiki Kaisha
Patent: US4725598 A1, 1988 ;
反应条件
ruthenium(IV) oxide; sodium periodate in water; ethyl acetate
0.166667 h; Ambient temperature;
参考文献
Mentlein, Rolf; Vowinkel, Erich
Liebigs Annalen der Chemie, 1984 , # 5 p. 1024 - 1035
反应条件
ruthenium(IV) oxide; sodium periodate in water; ethyl acetate
0.166667 h; Ambient temperature;
参考文献
Mentlein, Rolf; Vowinkel, Erich
Liebigs Annalen der Chemie, 1984 , # 5 p. 1024 - 1035
反应条件
oxygen in diethyl ether
Irradiation;
参考文献
Henning; Fuhrmann; Haupt; et al.
Pharmazie, 1982 , vol. 37, # 3 p. 224 - 225
