Alpha,Alpha-二甲基苄胺合成路线 （共 46 条）
参考文献
Zhurnal Russkago Fiziko-Khimicheskago Obshchestva, , vol. 26, p. 84
Chem. Zentralbl., , vol. 65, # II p. 33
反应条件
1: potassium carbonate / acetone / -10 - -5 °C 2: potassium carbonate / acetone / Ambient temperature View Scheme
参考文献
Omokawa; Ichizen; Takematsu
Agricultural and Biological Chemistry, 1987 , vol. 51, # 9 p. 2563 - 2568
反应条件
1: 95 percent / diethyl ether; hexane / 1.5 h / 20 °C 2: 90 percent / aq. NaOH; NaOCl / 20 °C 3: Thermolysis View Scheme
参考文献
Kornblum, Nathan; Fifolt, Michael J.
Tetrahedron, 1989 , vol. 45, # 5 p. 1311 - 1322
反应条件
1.1: s-BuLi; TMEDA / tetrahydrofuran / 2 h / -78 °C 1.2: 93 percent / tetrahydrofuran / cooling View Scheme
参考文献
Metallinos, Costa; Nerdinger, Sven; Snieckus, Victor
Organic Letters, 1999 , vol. 1, # 8 p. 1183 - 1186
反应条件
1-methyl-1H-imidazole; N,N,N',N,-tetramethylethylenediamine; potassium carbonate in chlorobenzene T=20 - 25°C; 2 h;
参考文献
Nakatsuji, Hidefumi; Morimoto, Mami; Misaki, Tomonori; Tanabe, Yoo
Tetrahedron, 2007 , vol. 63, # 48 p. 12071 - 12080
反应条件
peroxymonosulfuric acid; sodium carbonate in diethyl ether
参考文献
Klamann,D. et al.
Justus Liebigs Annalen der Chemie, 1965 , vol. 686, p. 122 - 133
参考文献
Baker; Ingold
Journal of the Chemical Society, 1927 , p. 262
参考文献
Baker; Ingold
Journal of the Chemical Society, 1927 , p. 262
反应条件
2: 96 percent / N-methylmorpholine, diphosgene / CH2Cl2 / 1 h / -30 °C View Scheme
参考文献
Kamer, Paul C. J.; Nolte, Roeland J. M.; Drenth, Wiendelt
Journal of the American Chemical Society, 1988 , vol. 110, # 20 p. 6818 - 6825
反应条件
potassium permanganate; magnesium sulfate in water; acetone
T=25 - 30°C; 46 h;
参考文献
Kornblum, Nathan; Fifolt, Michael J.
Tetrahedron, 1989 , vol. 45, # 5 p. 1311 - 1322
