4-(5-辛基嘧啶-2-基)苯酚合成路线 （共 3 条）
反应条件
sodium methylate in methanol
T=20°C; 14 h; Inert atmosphereReflux;
参考文献
Starkulla, Gundula F.; Klenk, Simon; Butschies, Martin; Tussetschlaeger, Stefan; Laschat, Sabine
Journal of Materials Chemistry, 2012 , vol. 22, # 41 p. 21987 - 21997,11
Title/Abstract Full Text Show Details
Starkulla, Gundula F.; Klenk, Simon; Butschies, Martin; Tussetschlaeger, Stefan; Laschat, Sabine
Journal of Materials Chemistry, 2012 , vol. 22, # 41 p. 21987 - 21997
反应条件
1.1: trichlorophosphate / 40 °C / |Inert atmosphere; |Cooling with ice
1.2: 2 h / 40 - 60 °C / |Inert atmosphere
2.1: sodium methylate / methanol / 14 h / 20 °C / |Inert atmosphere; |Reflux
View Scheme
参考文献
Starkulla, Gundula F.; Klenk, Simon; Butschies, Martin; Tussetschlaeger, Stefan; Laschat, Sabine
Journal of Materials Chemistry, 2012 , vol. 22, # 41 p. 21987 - 21997,11
Title/Abstract Full Text Show Details
Starkulla, Gundula F.; Klenk, Simon; Butschies, Martin; Tussetschlaeger, Stefan; Laschat, Sabine
Journal of Materials Chemistry, 2012 , vol. 22, # 41 p. 21987 - 21997
反应条件
potassium carbonate in cyclohexanone
T=80°C; 6 h;
参考文献
Yamaguchi, Akihisa; Nishiyama, Isa; Yamamoto, Jun; Yokoyama, Hiroshi; Yoshizawa, Atsushi
Journal of Materials Chemistry, 2005 , vol. 15, # 2 p. 280 - 288
