silica gel in melt Electrolysis; electrolysis of Na2CO3-K2CO3-SiO2 (5percent) melt (750°C, CO2 pressure 1 atm, current density not exceeding 0.2 A/cm, steel or Pt cathode); XRD, Auge spectroscopy, electron microscopy;
参考文献
Russian Journal of Applied Chemistry, , vol. 75, # 4 p. 562 - 564
in neat (no solvent) Electrochem. Process; eutectic mixture of 43.5 molpercent of Li2CO3, 31.5 molpercent of Na2CO3, and 25 molpercent of K2CO3, electrolytic reduction on Ni-electrode at 450°C; washed in HCl, dried in vac.;
参考文献
Journal of the Electrochemical Society, , vol. 149, # 5 p. D72-D78
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反应条件
byproducts: phosphor-carbon compound, CO; at starting red heat;
